Microextracción líquido-líquido dispersiva en la determinación de compuestos fenólicos en miel de abejas
Contenido principal del artículo
Resumen
Los componentes minoritarios en la miel de abejas constituyen una fuente nutricional y terapéutica para los seres humanos. Estos alcanzan más de 200 compuestos, y sus propiedades físico-químicas dependen del origen botánico y geográfico. Los compuestos fenólicos son productos naturales fitoquímicos del metabolismo secundario de las plantas. Estos son los responsables de la mayor parte de la actividad antioxidante en la miel de abejas. La determinación de los mismos es una pieza clave en la caracterización de las mieles, lo que incrementa el valor agregado de las mismas. En la actualidad, existen diferentes técnicas para la determinación de estos analitos en esta matriz apícola. Sin embargo, la microextracción líquido-líquido dispersiva resulta una técnica de preparación de muestras selectiva y sensible para la realización de este análisis. Los detectores que se emplean con frecuencia en el análisis de compuestos fenólicos son los espectrofotométricos (UV y arreglo de diodos) y de masas. Los analizadores de masas que se utilizan son el analizador de trampa de iones, el triple cuadrupolo, así como el analizador híbrido de masas Orbitrap.
Detalles del artículo
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